Exodus 9:24

9:24 Hail fell and fire mingled with the hail; the hail was so severe that there had not been any like it in all the land of Egypt since it had become a nation.

Exodus 10:14

10:14 The locusts went up over all the land of Egypt and settled down in all the territory of Egypt. It was very severe; there had been no locusts like them before, nor will there be such ever again.

Exodus 32:29

32:29 Moses said, “You have been consecrated today for the Lord, for each of you was against his son or against his brother, so he has given a blessing to you today.”

Exodus 34:34

34:34 But when Moses went in before the Lord to speak with him, he would remove the veil until he came out. Then he would come out and tell the Israelites what he had been commanded.