Exodus 7:14
The First Blow: Water to Blood
7:14 The Lord said to Moses, “Pharaoh’s heart is hard; he refuses to release the people.
Exodus 8:2
8:2 But if you refuse to release them, then I am going to plague all your territory with frogs.
Exodus 10:4
10:4 But if you refuse to release my people, I am going to bring locusts into your territory tomorrow.